Borthakur, M and Barthakur, M G and Boruah, R C (2008) Microwave promoted one-pot synthesis of novel A-ring fused steroidal dehydropiperazines. Steroids, 73 (5). pp. 539-542.

Preview

PDF (2570) - Published Version Download (306Kb) | Preview

Abstract

The preparation of ring-A fused steroidal dehydropiperazine at the 3,4-position is herein described. The novel steroidal dehydropiperazines were prepared from the annulation reaction of ethylenediamine with 3-keto-4-en steroids in a one-pot reaction under microwave irradiation. The key step involves base catalysed aerial oxidation of the C-6 methylene group followed by cyclocondensation of ethylenediamine via Michael addition reaction.

Item Type:	Article
Subjects:	Chemistry > Organic Chemistry
Divisions:	UNSPECIFIED
Depositing User:	Dr. PK Barooah
Date Deposited:	28 Dec 2011 05:50
Last Modified:	28 Dec 2011 05:50
URI:	http://neist.csircentral.net/id/eprint/123

Actions (login required)

View Item